::INDO AMERICAN JOURNAL OF PHARMACEUTICAL SCIENCES::

CODEN : IAJPBB
issn 2349-7750

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TITLE:

SYNTHESIS OF NEW MONONUCLEAR METAL COMPLEX OF MEDICINAL SIGNIFICANCE FROM HYDRAZONE SCHIFF BASE: SPECTROSCOPIC CHARACTERIZATION, AND ANTIMICROBIAL STUDY

AUTHORS:

Gajanan Dongare

ABSTRACT:

The [Zn(L)(H2O)]complex was synthesized by the condensation reaction of new medicinal significance hydrazone base ligand of 5-bromo-2-hydroxybenzylidene)-4-oxopiperidine-1-carbohydrazide (H2L). The complex was characterized by elemental and spectral techniques such as Infrared, UV-vis, and molar conductance, magnetic susceptibility, powder XRD. The ligand and metal stoichiometric ratio was found 1:1 (M:L) in the complex. The spectral, TG data shows tetrahedral geometry toward Zn (II) complex. X-ray diffraction study confirms nanocrystalline nature of metal complex. Keywords: Mononuclear, metal complex, spectral characterization, X-ray diffraction, Antimicrobial study.